bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

Base Information

Chemical Name:bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate
CAS No.:1312438-74-6
Molecular Formula:C₂₈H₃₈O₇Si
Molecular Weight:514.691
Hs Code.:

Synonyms:bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

Suppliers and Price of bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

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Technology Process of bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

There total 2 articles about bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

: 1312438-71-3
dimethyl (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

: 105-13-5
4-Methoxybenzyl alcohol

: 1312438-74-6
bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

Guidance literature:: oxo[hexa(trifluoroacetato)]tetrazinc; In di-isopropyl ether; at 80 ℃; Molecular sieve;

Reference yield:

: 1312438-70-2
dimethyl 2-hydroxy-4-methylenepentanedioate

: 1312438-74-6
bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-methyl-1H-imidazole / dichloromethane / 0 - 20 °C

2: oxo[hexa(trifluoroacetato)]tetrazinc / di-isopropyl ether / 80 °C / Molecular sieve

With 1-methyl-1H-imidazole; oxo[hexa(trifluoroacetato)]tetrazinc; In dichloromethane; di-isopropyl ether;