2,2,2-trichloroethyl 5-tert-butyl-3-(hydroxymethyl)-2-methoxyphenylcarbamate

Base Information

Chemical Name:2,2,2-trichloroethyl 5-tert-butyl-3-(hydroxymethyl)-2-methoxyphenylcarbamate
CAS No.:1283526-54-4
Molecular Formula:C₁₅H₂₀Cl₃NO₄
Molecular Weight:384.687
Hs Code.:

Synonyms:2,2,2-trichloroethyl 5-tert-butyl-3-(hydroxymethyl)-2-methoxyphenylcarbamate

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Chemical Property of 2,2,2-trichloroethyl 5-tert-butyl-3-(hydroxymethyl)-2-methoxyphenylcarbamate

Chemical Property:

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Technology Process of 2,2,2-trichloroethyl 5-tert-butyl-3-(hydroxymethyl)-2-methoxyphenylcarbamate

There total 4 articles about 2,2,2-trichloroethyl 5-tert-butyl-3-(hydroxymethyl)-2-methoxyphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1096697-99-2
(3-amino-5-(tert-butyl)-2-methoxyphenyl)methanol

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 1283526-54-4
2,2,2-trichloroethyl 5-tert-butyl-3-(hydroxymethyl)-2-methoxyphenylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 ℃; for 0.166667h;

Reference yield:

: 2725-53-3
2-hydroxy-5-t-butylbenzaldehyde

: 1283526-54-4
2,2,2-trichloroethyl 5-tert-butyl-3-(hydroxymethyl)-2-methoxyphenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitronium tetrafluoborate / acetonitrile / 1 h / -40 - -20 °C

1.2: 15 h / 20 °C

2.1: sodium tetrahydroborate / methanol / 0.25 h / 0 °C

2.2: 0.17 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 14 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.17 h / 0 °C

With sodium tetrahydroborate; nitronium tetrafluoborate; hydrogen; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethyl acetate; acetonitrile;

Reference yield:

: 99758-66-4
5-(tert-butyl)-2-methoxy-3-nitrobenzaldehyde

: 1283526-54-4
2,2,2-trichloroethyl 5-tert-butyl-3-(hydroxymethyl)-2-methoxyphenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / methanol / 0.25 h / 0 °C

1.2: 0.17 h / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 14 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.17 h / 0 °C

With sodium tetrahydroborate; hydrogen; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethyl acetate;