(1R,2S,5R)-(-)-menthyl (S)-4-methoxyphenylsulfinate

Base Information

Chemical Name:(1R,2S,5R)-(-)-menthyl (S)-4-methoxyphenylsulfinate
CAS No.:1942-34-3
Molecular Formula:C₁₇H₂₆O₃S
Molecular Weight:310.458
Hs Code.:

Synonyms:(1R,2S,5R)-(-)-menthyl (S)-4-methoxyphenylsulfinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,5R)-(-)-menthyl (S)-4-methoxyphenylsulfinate

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Technology Process of (1R,2S,5R)-(-)-menthyl (S)-4-methoxyphenylsulfinate

There total 12 articles about (1R,2S,5R)-(-)-menthyl (S)-4-methoxyphenylsulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 15356-60-2
(1S,2R,5S)-(+)-menthol

: 31401-23-7
p-methoxybenzenesulfinyl chloride

: 1942-34-3,98248-32-9,108293-21-6
(S_S)-(-)-menthyl-p-methoxybenzenesulfinate

Guidance literature:: With pyridine; In diethyl ether; 0 degC then allowed to warm to room temperature;
DOI:10.1016/S0040-4020(01)82425-X

Reference yield: 36.0%

: 2216-51-5
(-)-menthol

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 1942-34-3
(1R,2S,5R)-(-)-menthyl (S)-4-methoxyphenylsulfinate

Guidance literature:: With triethylamine; triphenylphosphine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.3762/bjoc.12.110

Reference yield: 11.0%

: 2216-51-5
(-)-menthol

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 1942-34-3
(1R,2S,5R)-(-)-menthyl (S)-4-methoxyphenylsulfinate

: S_S-l-menthyl p-methoxybenzenesulfinate

Guidance literature:: With triethylamine; triphenylphosphine; In dichloromethane; at 0 ℃; for 1h; Yield given; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(99)00066-X