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henicosan-4-one

Base Information
  • Chemical Name:henicosan-4-one
  • CAS No.:32822-45-0
  • Molecular Formula:C21H42O
  • Molecular Weight:310.564
  • Hs Code.:
henicosan-4-one

Synonyms:henicosan-4-one

Suppliers and Price of henicosan-4-one
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Chemical Property of henicosan-4-one
Chemical Property:
  • Vapor Pressure:0mmHg at 25°C 
Purity/Quality:
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MSDS Files:

SDS file from LookChem

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Technology Process of henicosan-4-one

There total 6 articles about henicosan-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
1-propylmagnesium chloride; With cerium(III) chloride; In tetrahydrofuran; at -78 ℃; for 2h;
4-(1-oxooctadecyl)morpholine; In tetrahydrofuran; at -78 ℃; for 1.5h; Further stages.;
DOI:10.1021/jo0263061
Guidance literature:
Multi-step reaction with 3 steps
1.1: thionyl chloride / benzene / 24 h / 50 °C
2.1: pyridine / CHCl3 / 20 h / 20 °C
3.1: CeCl3*7H2O / tetrahydrofuran / 2 h / -78 °C
3.2: 90 percent / tetrahydrofuran / 1.5 h / -78 °C
With pyridine; thionyl chloride; cerium(III) chloride; In tetrahydrofuran; chloroform; benzene;
DOI:10.1021/jo0263061
Guidance literature:
Multi-step reaction with 2 steps
1.1: pyridine / CHCl3 / 20 h / 20 °C
2.1: CeCl3*7H2O / tetrahydrofuran / 2 h / -78 °C
2.2: 90 percent / tetrahydrofuran / 1.5 h / -78 °C
With pyridine; cerium(III) chloride; In tetrahydrofuran; chloroform;
DOI:10.1021/jo0263061
upstream raw materials:

stearic acid

butyric acid

heneicosan-4-ol

4-(1-oxooctadecyl)morpholine

Downstream raw materials:

heneicosane

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