N-(2-bromophenyl)-3-methylbut-2-enamide

Base Information

Chemical Name:N-(2-bromophenyl)-3-methylbut-2-enamide
CAS No.:102804-45-5
Molecular Formula:C₁₁H₁₂BrNO
Molecular Weight:254.126
Hs Code.:
DSSTox Substance ID:DTXSID301278324
ChEMBL ID:CHEMBL1449545

Synonyms:N-(2-bromophenyl)-3-methyl-2-butenamide;2-Butenamide, N-(2-bromophenyl)-3-methyl-;102804-45-5;N-(2-bromophenyl)-3-methylbut-2-enamide;SMR000077070;MLS000050056;F3098-7451;CHEMBL1449545;DTXSID301278324;HMS2463C22;AKOS002253740;SDCCGMLS-0020729.P002;SR-01000278768;SR-01000278768-1;But-2-enoic acid, amide, 3-methyl-N-(2-bromophenyl)-

Suppliers and Price of N-(2-bromophenyl)-3-methylbut-2-enamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(2-bromophenyl)-3-methylbut-2-enamide

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:253.01023
Heavy Atom Count:14
Complexity:233

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CC(=O)NC1=CC=CC=C1Br)C

Technology Process of N-(2-bromophenyl)-3-methylbut-2-enamide

There total 1 articles about N-(2-bromophenyl)-3-methylbut-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 3350-78-5
3,3-Dimethylacryloyl chloride

: 615-36-1
2-bromoaniline

: 102804-45-5
N-(2-bromophenyl)-3-methylbut-2-enamide

Guidance literature:: With pyridine; In diethyl ether; at 0 - 20 ℃; for 1.25h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201911012

Reference yield: 98.0%

: 102804-45-5
N-(2-bromophenyl)-3-methylbut-2-enamide

: 74-88-4
methyl iodide

: 102804-49-9
N-(2-bromophenyl)-N,3-dimethylbut-2-enamide

Guidance literature:: With sodium hydride; In tetrahydrofuran; Ambient temperature;
DOI:10.1039/c39860000115

Reference yield: 91.0%

: 100-39-0
benzyl bromide

: 102804-45-5
N-(2-bromophenyl)-3-methylbut-2-enamide

: N-benzyl-N-(2-bromophenyl)-3-methylbut-2-enamide

Guidance literature:: N-(2-bromophenyl)-3-methylbut-2-enamide; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; Schlenk technique; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at 0 - 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201911012