α-bromocyclohexanecarboxaldehyde dimethylacetal

Base Information

Chemical Name:α-bromocyclohexanecarboxaldehyde dimethylacetal
CAS No.:90675-94-8
Molecular Formula:C₉H₁₇BrO₂
Molecular Weight:237.137
Hs Code.:

Synonyms:α-bromocyclohexanecarboxaldehyde dimethylacetal

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Chemical Property of α-bromocyclohexanecarboxaldehyde dimethylacetal

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Technology Process of α-bromocyclohexanecarboxaldehyde dimethylacetal

There total 3 articles about α-bromocyclohexanecarboxaldehyde dimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 18231-08-8
(dimethoxymethyl)cyclohexene

: 90675-94-8
α-bromocyclohexanecarboxaldehyde dimethylacetal

Guidance literature:: With chloro-trimethyl-silane; bromine; sodium bromide; In methanol; acetonitrile; at 40 ℃; for 0.5h;

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 90675-94-8
α-bromocyclohexanecarboxaldehyde dimethylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulphonic acid / methanol

2: 95 percent / Br₂, NaBr, chlorotrimethylsilane / acetonitrile; methanol / 0.5 h / 40 °C

With chloro-trimethyl-silane; bromine; toluene-4-sulfonic acid; sodium bromide; In methanol; acetonitrile;