N-Methylbenzohydrylamine hydrochloride

Base Information

• Chemical Name: N-Methylbenzohydrylamine hydrochloride
• CAS No.: 6268-97-9
• Molecular Formula: C₁₄H₁₅N*ClH
• Molecular Weight: 233.741
• European Community (EC) Number: 837-669-0
• NSC Number: 34675
• DSSTox Substance ID: DTXSID20388630
• Mol file: 6268-97-9.mol

Synonyms:N-Methylbenzohydrylamine hydrochloride;6268-97-9;N-methyl-1,1-diphenylmethanamine;hydrochloride;SCHEMBL2254912;NIOSH/DP6440000;DTXSID20388630;methylbenzhydrylamine hydrochloride;NSC34675;MFCD01732465;NSC-34675;LS-43402;(diphenylmethyl)(methyl)amine hydrochloride;N-Methyl-?-phenylbenzylamine hydrochloride;DP64400000;N-Methyl-alpha-phenylbenzylamine hydrochloride;EN300-6482771;Benzylamine, N-methyl-alpha-phenyl-, hydrochloride

Chemical Property of N-Methylbenzohydrylamine hydrochloride

Chemical Property:

• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 233.0971272
• Heavy Atom Count: 16
• Complexity: 148

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNC(C1=CC=CC=C1)C2=CC=CC=C2.Cl

Technology Process of N-Methylbenzohydrylamine hydrochloride

There total 1 articles about N-Methylbenzohydrylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzophenone (119-61-9) + methylamine (74-89-5) → benzhydryl-methyl-amine; hydrochloride (6268-97-9)

Guidance literature:

With hydrogenchloride; formic acid; magnesium chloride; Yield given. Multistep reaction; 1) water, a) 1h, 140-150 deg C b) 8h, reflux 2) MeOH reflux;

Reference yield:

benzhydryl-methyl-amine; hydrochloride (6268-97-9) → N-benzhydryl-N,S-dimethyl-isothiourea; hydriodide

Guidance literature:

Multi-step reaction with 2 steps

1: xylene

With xylene;

DOI:10.1021/ja01570a052

Reference yield:

ammonium thiocyanate (1147550-11-5) + benzhydryl-methyl-amine; hydrochloride (6268-97-9) → N-benzhydryl-N-methyl-thiourea (108897-18-3)

Guidance literature:

With xylene;

DOI:10.1021/ja01570a052

upstream raw materials:

benzophenone

methylamine

Downstream raw materials:

N-benzhydryl-N-methyl-thiourea