ethyl 2-(3-(3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate

Base Information

Chemical Name:ethyl 2-(3-(3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate
CAS No.:1292688-13-1
Molecular Formula:C₂₆H₃₈O₄Si
Molecular Weight:442.671
Hs Code.:

Synonyms:ethyl 2-(3-(3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate

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Chemical Property of ethyl 2-(3-(3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate

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Technology Process of ethyl 2-(3-(3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate

There total 10 articles about ethyl 2-(3-(3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 765302-48-5
ethyl 2-(3-hydroxy-4-methylphenyl)acetate

: 1292688-03-9
3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyl alcohol

: 1292688-13-1
ethyl 2-(3-(3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 4h;

Reference yield:

: 131236-69-6
methyl 2,6-dimethyl-3-hydroxybenzene-1-carboxylate

: 1292688-13-1
ethyl 2-(3-(3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 0 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 632-46-2
2,6-dimethylbenzoic acid

: 1292688-13-1
ethyl 2-(3-(3-(tert-butyldimethylsilyloxy)-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: nitric acid; sulfuric acid / nitromethane / 21 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

3.1: tin(II) chloride dihdyrate / ethanol / 2 h / 80 °C

3.2: pH 5

4.1: water; sodium nitrite; sulfuric acid / 0 - 120 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 0 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

7.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; tin(II) chloride dihdyrate; di-isopropyl azodicarboxylate; sulfuric acid; water; nitric acid; potassium carbonate; triphenylphosphine; sodium nitrite; In tetrahydrofuran; nitromethane; ethanol; N,N-dimethyl-formamide;