benzylamino-phenyl-acetaldehyde dimethylacetal

Base Information

• Chemical Name: benzylamino-phenyl-acetaldehyde dimethylacetal
• CAS No.: 101582-03-0
• Molecular Formula: C₁₇H₂₁NO₂
• Molecular Weight: 271.359
• Mol file: 101582-03-0.mol

Synonyms:benzylamino-phenyl-acetaldehyde dimethylacetal

Chemical Property of benzylamino-phenyl-acetaldehyde dimethylacetal

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzylamino-phenyl-acetaldehyde dimethylacetal

There total 1 articles about benzylamino-phenyl-acetaldehyde dimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethoxyacetaldehyde (51673-84-8) + benzylamine (100-46-9) → benzylamino-phenyl-acetaldehyde dimethylacetal (101582-03-0)

Guidance literature:

dimethoxyacetaldehyde; benzylamine; In toluene; at 20 ℃;

phenylmagnesium halide;

DOI:10.1007/s00726-011-1117-6

Reference yield: 53.0%

benzylamino-phenyl-acetaldehyde dimethylacetal (101582-03-0) + (4R,5R)-5-(methoxycarbonyl)-2,2-dimethyl-1,3-dioxolane-4-carboxylic acid (67812-33-3) → N-benzyl-N'-[(2,2-dimethoxy)-1-phenylethyl]-(2R,3R)-2,3-di-O-isopropylidenetartramic acid methyl ester

Guidance literature:

With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jo9904967

Reference yield:

benzylamino-phenyl-acetaldehyde dimethylacetal (101582-03-0) → rac-2,2-dimethoxy-1-phenylethanamine (57962-58-0)

Guidance literature:

With hydrogen; 5% Pd(II)/C(eggshell); In methanol; at 55 - 70 ℃; for 17h; under 15001.5 Torr;

upstream raw materials:

dimethoxyacetaldehyde

benzylamine

Downstream raw materials:

rac-2,2-dimethoxy-1-phenylethanamine

C₁₆H₁₅NO₃

(+/-)-benzyl 2-hydroxy-1-phenylethylcarbamate