Phosphoric acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester

Base Information

Chemical Name:Phosphoric acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester
CAS No.:183999-14-6
Molecular Formula:C₁₄H₂₁O₆P
Molecular Weight:316.291
Hs Code.:

Synonyms:Phosphoric acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester

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Chemical Property of Phosphoric acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester

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Technology Process of Phosphoric acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester

There total 3 articles about Phosphoric acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027989-03-2
Phosphorous acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester

: 183999-14-6
Phosphoric acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester

Guidance literature:: With tert.-butylhydroperoxide; In 2,2,4-trimethylpentane; dichloromethane; at 0 - 25 ℃; for 2h; Yield given;
DOI:10.1021/jm960434y

Reference yield:

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 183999-14-6
Phosphoric acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N,N-diiisopropylethylamine / 1.) CH₂Cl₂, -78 deg C, 1 h, 2.) CH₂Cl₂, from -78 deg C to 25 deg C, 2 h

2: t-BuOOH / CH₂Cl₂; 2,2,4-trimethyl-pentane / 2 h / 0 - 25 °C

With tert.-butylhydroperoxide; N-ethyl-N,N-diisopropylamine; In 2,2,4-trimethylpentane; dichloromethane;
DOI:10.1021/jm960434y

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 183999-14-6
Phosphoric acid benzyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N,N-diiisopropylethylamine / 1.) CH₂Cl₂, -78 deg C, 1 h, 2.) CH₂Cl₂, from -78 deg C to 25 deg C, 2 h

2: t-BuOOH / CH₂Cl₂; 2,2,4-trimethyl-pentane / 2 h / 0 - 25 °C

With tert.-butylhydroperoxide; N-ethyl-N,N-diisopropylamine; In 2,2,4-trimethylpentane; dichloromethane;
DOI:10.1021/jm960434y