1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane

Base Information

Chemical Name:1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane
CAS No.:1326316-88-4
Molecular Formula:C₂₄H₅₄Cl₂Sn₃
Molecular Weight:769.729
Hs Code.:

Synonyms:1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane

Chemical Property:

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Technology Process of 1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane

There total 2 articles about 1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 677-22-5
tert-butylmagnesium chloride

: 7646-78-8
tin(IV) chloride

: 1326316-88-4
1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane

: 19429-30-2
di-tert-butyltin dichloride

: 7529-39-7
octa-tert.butyl-cyclotetrastannane

Guidance literature:: In tetrahydrofuran; hexane; a THF soln. of Mg compd. added to SnCl4 in hexane; recrystd. (hexanes);
DOI:10.1021/om200548s

Reference yield:

: 677-22-5
tert-butylmagnesium chloride

: 7646-78-8
tin(IV) chloride

: 1326316-88-4
1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane

: 52313-26-5
1,2-dichloro-1,1,2,2-tetra-tert-butyldistannane

: 19429-30-2
di-tert-butyltin dichloride

Guidance literature:: In tetrahydrofuran; benzene; a THF soln. of Mg compd. added to SnCl4 in C6H6;
DOI:10.1021/om200548s

Reference yield: 2.0%

: 1326316-88-4
1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane

: 1145-98-8
1,2-diphenyltetramethyldisilane

: C₃₂H₆₅ClSiSn₃

Guidance literature:: 1,2-diphenyltetramethyldisilane; With lithium; In tetrahydrofuran; Inert atmosphere; Schlenk technique;

1,3-dichloro-1,1,2,2,3,3-hexa-tert-butyltristannane; In tetrahydrofuran; hexane; at -25 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.ica.2017.03.045