{3-[2-(difluoromethyl)-5-methyl-4-nitrophenoxy]propyl}(trimethyl)silane

Base Information

Chemical Name:{3-[2-(difluoromethyl)-5-methyl-4-nitrophenoxy]propyl}(trimethyl)silane
CAS No.:1029557-22-9
Molecular Formula:C₁₄H₂₁F₂NO₃Si
Molecular Weight:317.408
Hs Code.:

Synonyms:{3-[2-(difluoromethyl)-5-methyl-4-nitrophenoxy]propyl}(trimethyl)silane

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Chemical Property of {3-[2-(difluoromethyl)-5-methyl-4-nitrophenoxy]propyl}(trimethyl)silane

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Technology Process of {3-[2-(difluoromethyl)-5-methyl-4-nitrophenoxy]propyl}(trimethyl)silane

There total 3 articles about {3-[2-(difluoromethyl)-5-methyl-4-nitrophenoxy]propyl}(trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2917-47-7
3-trimethylsilyl-1-propanol

: 1029557-20-7
1-bromo-2-(difluoromethyl)-5-methyl-4-nitrobenzene

: 1029557-22-9
{3-[2-(difluoromethyl)-5-methyl-4-nitrophenoxy]propyl}(trimethyl)silane

Guidance literature:: 3-trimethylsilyl-1-propanol; 1-bromo-2-(difluoromethyl)-5-methyl-4-nitrobenzene; With caesium carbonate; In toluene; for 0.166667h;

With johnphos; palladium diacetate; In toluene; at 20 - 90 ℃; for 12.1667h;

Reference yield:

: 824-54-4
2-bromo-4-methylbenzaldehyde

: 1029557-22-9
{3-[2-(difluoromethyl)-5-methyl-4-nitrophenoxy]propyl}(trimethyl)silane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; nitric acid / 1 h / 5 - 15 °C

2.1: diethylamino-sulfur trifluoride / dichloromethane / 2 h / -30 - 20 °C

3.1: caesium carbonate / toluene / 0.17 h

3.2: 12.17 h / 20 - 90 °C

With diethylamino-sulfur trifluoride; sulfuric acid; nitric acid; caesium carbonate; In dichloromethane; toluene;

Reference yield:

: 159730-72-0
2-bromo-4-methyl-5-nitrobenzaldehyde

: 1029557-22-9
{3-[2-(difluoromethyl)-5-methyl-4-nitrophenoxy]propyl}(trimethyl)silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethylamino-sulfur trifluoride / dichloromethane / 2 h / -30 - 20 °C

2.1: caesium carbonate / toluene / 0.17 h

2.2: 12.17 h / 20 - 90 °C

With diethylamino-sulfur trifluoride; caesium carbonate; In dichloromethane; toluene;