(4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine

Base Information

Chemical Name:(4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine
CAS No.:102832-01-9
Molecular Formula:C₁₉H₂₉NO₃Si
Molecular Weight:347.53
Hs Code.:

Synonyms:(4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine

Suppliers and Price of (4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine

There total 4 articles about (4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 102831-99-2
(4S)-1-(tert-Butyldimethylsilyl)-4-<(1R)-1-<((4S)-4-ethyl-2-thioxo-1,3-thiazolidin-3-yl)carbonyl>ethyl>azetidin-2-one

: 20194-18-7
sodium phenyl-methanolate

: 102832-01-9
(4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine

Guidance literature:: In toluene; 0 deg C, 1 h, than rt., 30 min;
DOI:10.1021/ja00275a082

Reference yield:

: 102831-94-7
(4S)-4-<(1R)-1-<((4S)-4-Ethyl-2-thioxo-1,3-thiazolidin-3-yl)carbonyl>ethyl>azetidin-2-one

: 102832-01-9
(4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Et₃N / dimethylformamide / 0 °C

2: 40 percent / toluene / 0 deg C, 1 h, than rt., 30 min

With triethylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja00275a082

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 102832-01-9
(4S)-4-<(1R)-1-(benzyloxycarbonyl)ethyl>-1-(tert-butyldimethylsilyl)-2-oxoazetidine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Et₃N / dimethylformamide / 0 °C

2: 40 percent / toluene / 0 deg C, 1 h, than rt., 30 min

With triethylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja00275a082