5'-O-(4-chlorophenoxyacetyl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine

Base Information

Chemical Name:5'-O-(4-chlorophenoxyacetyl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine
CAS No.:82892-70-4
Molecular Formula:C₃₃H₃₀ClN₅O₈
Molecular Weight:660.083
Hs Code.:

Synonyms:5'-O-(4-chlorophenoxyacetyl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine

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Chemical Property of 5'-O-(4-chlorophenoxyacetyl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine

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Technology Process of 5'-O-(4-chlorophenoxyacetyl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine

There total 2 articles about 5'-O-(4-chlorophenoxyacetyl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 82892-59-9
6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine

: 4122-68-3
4-chlorophenyloxyacetyl chloride

: 82892-70-4
5'-O-(4-chlorophenoxyacetyl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine

Guidance literature:: In pyridine; acetonitrile; for 2h; Ambient temperature;
DOI:10.1021/ja00385a026

Reference yield:

: 82995-92-4
{6-Benzyloxy-9-[(2R,4S,5R)-4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-9H-purin-2-yl}-carbamic acid benzyl ester

: 82892-70-4
5'-O-(4-chlorophenoxyacetyl)-6-O-benzyl-2-N-(benzyloxycarbonyl)-2'-deoxyguanosine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammonium fluoride / tetrahydrofuran

2: 84 percent / acetonitrile; pyridine / 2 h / Ambient temperature

With tetrabutyl ammonium fluoride; In tetrahydrofuran; pyridine; acetonitrile;
DOI:10.1021/ja00385a026