5-chloro-N-(3-chloropropyl)-2-{[2-(trifluoromethyl)phenyl]thio}aniline

Base Information

Chemical Name:5-chloro-N-(3-chloropropyl)-2-{[2-(trifluoromethyl)phenyl]thio}aniline
CAS No.:1100794-82-8
Molecular Formula:C₁₆H₁₄Cl₂F₃NS
Molecular Weight:380.261
Hs Code.:

Synonyms:5-chloro-N-(3-chloropropyl)-2-{[2-(trifluoromethyl)phenyl]thio}aniline

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Chemical Property of 5-chloro-N-(3-chloropropyl)-2-{[2-(trifluoromethyl)phenyl]thio}aniline

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Technology Process of 5-chloro-N-(3-chloropropyl)-2-{[2-(trifluoromethyl)phenyl]thio}aniline

There total 1 articles about 5-chloro-N-(3-chloropropyl)-2-{[2-(trifluoromethyl)phenyl]thio}aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1100794-68-0
5-chloro-2-{[2-(trifluoromethyl)phenyl]thio}aniline

: 625-36-5
2-chloropropionyl chloride

: 1100794-82-8
5-chloro-N-(3-chloropropyl)-2-{[2-(trifluoromethyl)phenyl]thio}aniline

Guidance literature:: 5-chloro-2-{[2-(trifluoromethyl)phenyl]thio}aniline; 2-chloropropionyl chloride; With pyridine; In tetrahydrofuran; at 25 ℃; for 1.5h; Inert atmosphere;

With borane-THF; In tetrahydrofuran; at 67 ℃; for 2h; Inert atmosphere;
DOI:10.1039/b806371k

Reference yield: 96.0%

: 1100794-82-8
5-chloro-N-(3-chloropropyl)-2-{[2-(trifluoromethyl)phenyl]thio}aniline

: 124-40-3
dimethyl amine

: 1100795-04-7
N'-(5-chloro-2-{[2-(trifluoromethyl)phenyl]thio}phenyl)-N,N-dimethylpropan-1,3-diamine

Guidance literature:: In water; N,N-dimethyl-formamide; at 90 ℃; Inert atmosphere;
DOI:10.1039/b806371k

Reference yield: 77.0%

: 109-01-3
1-methyl-piperazine

: 1100794-82-8
5-chloro-N-(3-chloropropyl)-2-{[2-(trifluoromethyl)phenyl]thio}aniline

: 1100794-92-0
5-chloro-N-[3-(4-methylpiperazin-1-yl)propyl]-2-{[2-(trifluoromethyl)phenyl]thio}aniline

Guidance literature:: With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 80 - 120 ℃; for 1.16667h; Microwave irradiation; Inert atmosphere;
DOI:10.1039/b806371k