C₂₆H₂₆N₂O₂

Base Information

• Chemical Name: C₂₆H₂₆N₂O₂
• CAS No.: 1320267-54-6
• Molecular Formula: C₂₆H₂₆N₂O₂
• Molecular Weight: 398.505
• Mol file: 1320267-54-6.mol

Synonyms:C₂₆H₂₆N₂O₂

Chemical Property of C₂₆H₂₆N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₆N₂O₂

There total 2 articles about C₂₆H₂₆N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

methanol (67-56-1) + phosgene (75-44-5) + C24H22N2 → C26H26N2O2 (1320267-54-6)

Guidance literature:

phosgene; C₂₄H₂₂N₂; With triethylamine; In toluene; at -45 - 23 ℃;

methanol; In toluene; at -30 - 23 ℃;

With palladium on activated charcoal; hydrogen; In ethanol; ethyl acetate; toluene; at 0 ℃;

DOI:10.1038/nature10232

Reference yield:

C27H28N2O3 (1320267-61-5) → C26H26N2O2 (1320267-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trimethylsilyl iodide; triethylamine / dichloromethane / 0 °C

1.2: 40 °C

1.3: 0 °C

2.1: triethylamine / toluene / -45 - 23 °C

2.2: -30 - 23 °C

2.3: 0 °C

With trimethylsilyl iodide; triethylamine; In dichloromethane; toluene;

DOI:10.1038/nature10232

Reference yield: 86.0%

PVS (5535-48-8) + C26H26N2O2 (1320267-54-6) → C34H34N2O4S (1320267-57-9)

Guidance literature:

In benzene; at 100 ℃;

DOI:10.1038/nature10232

upstream raw materials:

methanol

phosgene

C₂₇H₂₈N₂O₃

Downstream raw materials:

C₃₄H₃₄N₂O₄S

kopsinine