(1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime

Base Information

Chemical Name:(1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime
CAS No.:1356600-18-4
Molecular Formula:C₁₆H₁₆FNO₃
Molecular Weight:289.306
Hs Code.:

Synonyms:(1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime

Suppliers and Price of (1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime

There total 5 articles about (1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.34%

: 1356600-17-3
3-fluoro-4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzaldehyde

: 1356600-18-4
(1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime

Guidance literature:: With methanol; sodium tetrahydroborate; at 0 ℃; for 0.5h;

Reference yield:

: 31376-92-8
(1E,1Z)-2-bromo-N-methoxy-1-phenylethanimine

: 96740-93-1
3-fluoro-4-hydroxybenzyl alcohol

: 1356600-18-4
(1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime

Guidance literature:: With potassium carbonate; In acetone; at 45 ℃; for 12h;
DOI:10.1039/c6ra07356e

Reference yield:

: 351-54-2
3-fluoro-p-anisaldehyde

: 1356600-18-4
(1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron tribromide / dichloromethane / 18 h / -78 - 20 °C

1.2: 0 °C

2.1: potassium carbonate / acetonitrile / 4 h / 0 - 85 °C / Inert atmosphere

3.1: sodium tetrahydroborate; methanol / 0.5 h / 0 °C

With methanol; sodium tetrahydroborate; boron tribromide; potassium carbonate; In dichloromethane; acetonitrile;