(1E,1Z)-2-[4-(bromomethyl)-2-fluorophenoxy]-1-phenylethanone O-methyloxime

Base Information

Chemical Name:(1E,1Z)-2-[4-(bromomethyl)-2-fluorophenoxy]-1-phenylethanone O-methyloxime
CAS No.:1356600-19-5
Molecular Formula:C₁₆H₁₅BrFNO₂
Molecular Weight:352.203
Hs Code.:

Synonyms:(1E,1Z)-2-[4-(bromomethyl)-2-fluorophenoxy]-1-phenylethanone O-methyloxime

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Chemical Property of (1E,1Z)-2-[4-(bromomethyl)-2-fluorophenoxy]-1-phenylethanone O-methyloxime

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Technology Process of (1E,1Z)-2-[4-(bromomethyl)-2-fluorophenoxy]-1-phenylethanone O-methyloxime

There total 6 articles about (1E,1Z)-2-[4-(bromomethyl)-2-fluorophenoxy]-1-phenylethanone O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.44%

: 1356600-18-4
(1E,1Z)-2-[2-fluoro-4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime

: 1356600-19-5
(1E,1Z)-2-[4-(bromomethyl)-2-fluorophenoxy]-1-phenylethanone O-methyloxime

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1356600-19-5
(1E,1Z)-2-[4-(bromomethyl)-2-fluorophenoxy]-1-phenylethanone O-methyloxime

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate; acetic acid / 0.08 h / 20 °C

1.2: 3 h / 20 - 80 °C

2.1: potassium carbonate / acetonitrile / 4 h / 0 - 85 °C / Inert atmosphere

3.1: sodium tetrahydroborate; methanol / 0.5 h / 0 °C

4.1: phosphorus tribromide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; sodium acetate; phosphorus tribromide; potassium carbonate; acetic acid; In dichloromethane; acetonitrile;

Reference yield:

: 351-54-2
3-fluoro-p-anisaldehyde

: 1356600-19-5
(1E,1Z)-2-[4-(bromomethyl)-2-fluorophenoxy]-1-phenylethanone O-methyloxime

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron tribromide / dichloromethane / 18 h / -78 - 20 °C

1.2: 0 °C

2.1: potassium carbonate / acetonitrile / 4 h / 0 - 85 °C / Inert atmosphere

3.1: sodium tetrahydroborate; methanol / 0.5 h / 0 °C

4.1: phosphorus tribromide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; boron tribromide; phosphorus tribromide; potassium carbonate; In dichloromethane; acetonitrile;