5-(methanesulphonyl-methyl-amino)-isophthalic acid mono-tert-butyl ester

Base Information

Chemical Name:5-(methanesulphonyl-methyl-amino)-isophthalic acid mono-tert-butyl ester
CAS No.:1079398-49-4
Molecular Formula:C₁₄H₁₉NO₆S
Molecular Weight:329.374
Hs Code.:

Synonyms:5-(methanesulphonyl-methyl-amino)-isophthalic acid mono-tert-butyl ester

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Chemical Property of 5-(methanesulphonyl-methyl-amino)-isophthalic acid mono-tert-butyl ester

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Technology Process of 5-(methanesulphonyl-methyl-amino)-isophthalic acid mono-tert-butyl ester

There total 3 articles about 5-(methanesulphonyl-methyl-amino)-isophthalic acid mono-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 695215-94-2
3-(methoxycarbonyl)-5-[methyl(methylsulfonyl)amino]benzoic acid

: 1079398-49-4
5-(methanesulphonyl-methyl-amino)-isophthalic acid mono-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0 - 20 °C

2.1: sodium hydroxide; water / tetrahydrofuran; methanol / 3.5 h / 0 - 20 °C

2.2: 0 °C / pH 2

With dmap; sodium hydroxide; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 99-27-4
dimethyl 5-aminoisophthalate

: 1079398-49-4
5-(methanesulphonyl-methyl-amino)-isophthalic acid mono-tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / dichloromethane / 4 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 20 °C

3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 8.5 h / 0 - 20 °C

4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0 - 20 °C

5.1: sodium hydroxide; water / tetrahydrofuran; methanol / 3.5 h / 0 - 20 °C

5.2: 0 °C / pH 2

With pyridine; dmap; sodium hydroxide; water; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 62814-45-3
5-methanesulphonylamino-isophthalic acid dimethyl ester

: 1079398-49-4
5-(methanesulphonyl-methyl-amino)-isophthalic acid mono-tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 20 °C

2.1: sodium hydroxide; water / tetrahydrofuran; methanol / 8.5 h / 0 - 20 °C

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0 - 20 °C

4.1: sodium hydroxide; water / tetrahydrofuran; methanol / 3.5 h / 0 - 20 °C

4.2: 0 °C / pH 2

With dmap; sodium hydroxide; water; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;