4,5,6,7-tetrachloro-2,2-dihydro-2,2,2-triphenyl-1,3,2-benzodioxastibole

Base Information

Chemical Name:4,5,6,7-tetrachloro-2,2-dihydro-2,2,2-triphenyl-1,3,2-benzodioxastibole
CAS No.:86780-29-2
Molecular Formula:C₂₄H₁₅Cl₄O₂Sb
Molecular Weight:598.944
Hs Code.:

Synonyms:4,5,6,7-tetrachloro-2,2-dihydro-2,2,2-triphenyl-1,3,2-benzodioxastibole

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Chemical Property of 4,5,6,7-tetrachloro-2,2-dihydro-2,2,2-triphenyl-1,3,2-benzodioxastibole

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Technology Process of 4,5,6,7-tetrachloro-2,2-dihydro-2,2,2-triphenyl-1,3,2-benzodioxastibole

There total 3 articles about 4,5,6,7-tetrachloro-2,2-dihydro-2,2,2-triphenyl-1,3,2-benzodioxastibole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2435-53-2
o-tetrachloroquinone

: triphenylstibine sulfide

: 86780-29-2
4,5,6,7-tetrachloro-2,2-dihydro-2,2,2-triphenyl-1,3,2-benzodioxastibole

Guidance literature:: In benzene; byproducts: sulfur; refluxing (10 h); standing (room temp, 12 h), removal of solvent (vac.), washing (EtOH, CS2), filtration off, recrystn. (CHCl3/petroleum ether); elem. anal.;

Reference yield: 80.0%

: 2435-53-2
o-tetrachloroquinone

: 603-36-1
triphenylantimony

: 86780-29-2
4,5,6,7-tetrachloro-2,2-dihydro-2,2,2-triphenyl-1,3,2-benzodioxastibole

Guidance literature:: In benzene; room temp., 12 h; removal of solvent (vac.), trituration (petroleum ether), recrystn. (CHCl3/petroleum ether);

Reference yield:

: 2435-53-2
o-tetrachloroquinone

: Sb⁽³⁺⁾*3C₆H₅^(1-)=Sb(C₆H₅)3

: 86780-29-2
4,5,6,7-tetrachloro-2,2-dihydro-2,2,2-triphenyl-1,3,2-benzodioxastibole

Guidance literature:: In toluene; atm. of dry N2; dropwise addn. of Sb(C6H5)3 in toluene to toluene soln. of o-quinone; stirring (4 h); mechanism discussed (ESR-data);; pptn. of colorless solid (concn. in vac./addn. of light petroleum); drying (vac.); elem. anal;;
DOI:10.1039/DT9930001381