C₅₅H₇₃NO₁₄Si

Base Information

Chemical Name:C₅₅H₇₃NO₁₄Si
CAS No.:175444-23-2
Molecular Formula:C₅₅H₇₃NO₁₄Si
Molecular Weight:1000.27
Hs Code.:

C<sub>55</sub>H<sub>73</sub>NO<sub>14</sub>Si

Synonyms:C₅₅H₇₃NO₁₄Si

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Chemical Property of C₅₅H₇₃NO₁₄Si

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Technology Process of C₅₅H₇₃NO₁₄Si

There total 6 articles about C₅₅H₇₃NO₁₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 155396-69-3
(2R,4S,5R)-(2R,4S,5R)-3-tert-butoxycarbonyl-2-(4-methoxyphenyl)-4-phenyl-1,3-oxazolidine-5-carboxylic acid

: 175444-20-9
C₃₃H₅₀O₉Si

: 175444-23-2
C₅₅H₇₃NO₁₄Si

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In toluene; at 60 ℃;
DOI:10.1016/0040-4039(96)00117-7

Reference yield:

: 144654-43-3
4,10-bis(deacetyl)-7-(triethylsily)baccatin III

: 175444-23-2
C₅₅H₇₃NO₁₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / PCC, pyridine / Ambient temperature

2: 50 percent / Zn, NH₄OH, NH₄Cl / ethyl acetate / Ambient temperature

3: 60 percent / NaBH₄ / methanol

4: 62 percent / DCC, DMAP / toluene / 60 °C

With pyridine; dmap; ammonium hydroxide; sodium tetrahydroborate; ammonium chloride; dicyclohexyl-carbodiimide; pyridinium chlorochromate; zinc; In methanol; ethyl acetate; toluene;
DOI:10.1016/0040-4039(96)00117-7

Reference yield:

: 115437-18-8
7-triethylsilyl-10-deacetylbaccatin III

: 175444-23-2
C₅₅H₇₃NO₁₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / LiBHEt₃ / tetrahydrofuran / -78 °C

2: 72 percent / PCC, pyridine / Ambient temperature

3: 50 percent / Zn, NH₄OH, NH₄Cl / ethyl acetate / Ambient temperature

4: 60 percent / NaBH₄ / methanol

5: 62 percent / DCC, DMAP / toluene / 60 °C

With pyridine; dmap; ammonium hydroxide; sodium tetrahydroborate; lithium triethylborohydride; ammonium chloride; dicyclohexyl-carbodiimide; pyridinium chlorochromate; zinc; In tetrahydrofuran; methanol; ethyl acetate; toluene;
DOI:10.1016/0040-4039(96)00117-7