1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)-6-formylbenzene

Base Information

Chemical Name:1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)-6-formylbenzene
CAS No.:528869-14-9
Molecular Formula:C₁₃H₁₂F₄O₃
Molecular Weight:292.23
Hs Code.:

Synonyms:1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)-6-formylbenzene

Suppliers and Price of 1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)-6-formylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)-6-formylbenzene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)-6-formylbenzene

There total 2 articles about 1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)-6-formylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 109-94-4
formic acid ethyl ester

: 528869-08-1
1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)benzene

: 528869-14-9
1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)-6-formylbenzene

Guidance literature:: 1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)benzene; With n-butyllithium; In tetrahydrofuran; at -60 ℃; for 0.25h;

formic acid ethyl ester; In tetrahydrofuran; at -60 - 20 ℃;
DOI:10.1016/S0022-1139(02)00289-0

Reference yield:

: 19842-76-3
2,3,5,6-tetrafluorobenzaldehyde

: 528869-14-9
1,2,4,5-tetrafluoro-3-(5,5-dimethyl-1,3-dioxan-2-yl)-6-formylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 67 g / p-TsOH / toluene / 1 h / Heating

2.1: n-BuLi / tetrahydrofuran / 0.25 h / -60 °C

2.2: 73 percent / tetrahydrofuran / -60 - 20 °C

With n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1016/S0022-1139(02)00289-0