dibenzyl 3,4'-bis(2-hydroxyethyl)-4,3'-dimethylpyrromethane-5,5'-di-carboxylate

Base Information

Chemical Name:dibenzyl 3,4'-bis(2-hydroxyethyl)-4,3'-dimethylpyrromethane-5,5'-di-carboxylate
CAS No.:87377-78-4
Molecular Formula:C₃₁H₃₄N₂O₆
Molecular Weight:530.621
Hs Code.:

Synonyms:dibenzyl 3,4'-bis(2-hydroxyethyl)-4,3'-dimethylpyrromethane-5,5'-di-carboxylate

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Chemical Property of dibenzyl 3,4'-bis(2-hydroxyethyl)-4,3'-dimethylpyrromethane-5,5'-di-carboxylate

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Technology Process of dibenzyl 3,4'-bis(2-hydroxyethyl)-4,3'-dimethylpyrromethane-5,5'-di-carboxylate

There total 3 articles about dibenzyl 3,4'-bis(2-hydroxyethyl)-4,3'-dimethylpyrromethane-5,5'-di-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 87377-77-3
dibenzyl 3-ethoxycarbonylmethyl-4'-methoxycarbonylmethyl-4,3'-dimethylpyrromethane-5,5'-dicarboxylate

: 87377-78-4
dibenzyl 3,4'-bis(2-hydroxyethyl)-4,3'-dimethylpyrromethane-5,5'-di-carboxylate

Guidance literature:: With diborane; In tetrahydrofuran; for 4.5h;
DOI:10.1016/S0040-4020(01)88698-1

Reference yield:

: 75630-46-5
benzyl 5-acetoxymethyl-3-(methoxycarbonylmethyl)-4-methylpyrrole-2-carboxylate

: 87377-78-4
dibenzyl 3,4'-bis(2-hydroxyethyl)-4,3'-dimethylpyrromethane-5,5'-di-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / SnCl₄ / CH₂Cl₂ / 1.5 h / -10 - 0 °C

2: 90 percent / diborane / tetrahydrofuran / 4.5 h

With tin(IV) chloride; diborane; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)88698-1

Reference yield:

: 87377-76-2
benzyl 4-ethoxycarbonylmethyl-3-methylpyrrole-2-carboxylate

: 87377-78-4
dibenzyl 3,4'-bis(2-hydroxyethyl)-4,3'-dimethylpyrromethane-5,5'-di-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / SnCl₄ / CH₂Cl₂ / 1.5 h / -10 - 0 °C

2: 90 percent / diborane / tetrahydrofuran / 4.5 h

With tin(IV) chloride; diborane; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)88698-1