methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate

Base Information

Chemical Name:methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate
CAS No.:1167416-56-9
Molecular Formula:C₁₅H₂₀BrNO₅
Molecular Weight:374.232
Hs Code.:

Synonyms:methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate

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Chemical Property of methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate

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Technology Process of methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate

There total 2 articles about methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 26690-80-2
2-(N-tert-butoxycarbonylamino)ethanol

: 4068-76-2
5-bromo-2-hydroxy-benzoic acid methyl ester

: 1167416-56-9
methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 18.5h;
DOI:10.1021/jm5010336

Reference yield:

: 2-(tert-butoxycarbonylamino)ethyl benzenesulfonate

: 4068-76-2
5-bromo-2-hydroxy-benzoic acid methyl ester

: 1167416-56-9
methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 35 ℃; for 24h;

Reference yield: 59.0%

: 1167416-56-9
methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate

: 5755-05-5
7-bromo-3,4-dihydrobenzo[f][1,4]oxazepin-5(2H)-one

Guidance literature:: methyl 5-bromo-2-{[2-({[(1,1-dimethylethyl)oxy]carbonyl}amino)ethyl]oxy}benzoate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 21h;

With triethylamine; In toluene; at 100 ℃; for 16h;
DOI:10.1021/jm5010336