Technology Process of C22H14F7NO2
There total 4 articles about C22H14F7NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
palladium bis[bis(diphenylphosphino)ferrocene] dichloride;
In
tetrahydrofuran; water;
at 20 - 70 ℃;
for 2h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper / dimethyl sulfoxide / 1 h / 20 °C
1.2: 15 h / 20 °C
2.1: n-butyllithium / diethyl ether / 3 h / -70 - 20 °C
3.1: diethyl ether / 2 h / 0 - 20 °C
4.1: potassium carbonate / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / water; tetrahydrofuran / 2 h / 20 - 70 °C / Inert atmosphere
With
n-butyllithium; copper; potassium carbonate;
palladium bis[bis(diphenylphosphino)ferrocene] dichloride;
In
tetrahydrofuran; diethyl ether; water; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium / diethyl ether / 3 h / -70 - 20 °C
2: diethyl ether / 2 h / 0 - 20 °C
3: potassium carbonate / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / water; tetrahydrofuran / 2 h / 20 - 70 °C / Inert atmosphere
With
n-butyllithium; potassium carbonate;
palladium bis[bis(diphenylphosphino)ferrocene] dichloride;
In
tetrahydrofuran; diethyl ether; water;