2-methyl-1-<5-(2-methylphenyl)-1,3,4-thiadiazol-2-yl>isothiourea hydroiodide

Base Information

Chemical Name:2-methyl-1-<5-(2-methylphenyl)-1,3,4-thiadiazol-2-yl>isothiourea hydroiodide
CAS No.:113113-22-7
Molecular Formula:C₁₁H₁₂N₄S₂*HI
Molecular Weight:392.288
Hs Code.:

Synonyms:2-methyl-1-<5-(2-methylphenyl)-1,3,4-thiadiazol-2-yl>isothiourea hydroiodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl-1-<5-(2-methylphenyl)-1,3,4-thiadiazol-2-yl>isothiourea hydroiodide

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Technology Process of 2-methyl-1-<5-(2-methylphenyl)-1,3,4-thiadiazol-2-yl>isothiourea hydroiodide

There total 2 articles about 2-methyl-1-<5-(2-methylphenyl)-1,3,4-thiadiazol-2-yl>isothiourea hydroiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 113113-21-6
N-<5-(2-methylphenyl)-1,3,4-thiadiazol-2-yl>thiourea

: 74-88-4
methyl iodide

: 113113-22-7
2-methyl-1-<5-(2-methylphenyl)-1,3,4-thiadiazol-2-yl>isothiourea hydroiodide

Guidance literature:: In ethanol; for 3h; Heating;
DOI:10.1021/jm00400a004

Reference yield:

: 59565-54-7
5-(2-methylphenyl)-1,3,4-thiadiazol-2-amine

: 113113-22-7
2-methyl-1-<5-(2-methylphenyl)-1,3,4-thiadiazol-2-yl>isothiourea hydroiodide

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) 2N NaOH / 1.) toluene, reflux, 1.5 h, 2.) heating, 2 h

2: 20 percent / ethanol / 3 h / Heating

With sodium hydroxide; In ethanol;
DOI:10.1021/jm00400a004