2-benzyloxy-6-methoxycarbonylphenyl 2-benzyloxy-6-methoxy-4-methoxycarbonylphenyl ketone

Base Information

Chemical Name:2-benzyloxy-6-methoxycarbonylphenyl 2-benzyloxy-6-methoxy-4-methoxycarbonylphenyl ketone
CAS No.:171009-39-5
Molecular Formula:C₃₂H₂₈O₈
Molecular Weight:540.57
Hs Code.:

Synonyms:2-benzyloxy-6-methoxycarbonylphenyl 2-benzyloxy-6-methoxy-4-methoxycarbonylphenyl ketone

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Chemical Property of 2-benzyloxy-6-methoxycarbonylphenyl 2-benzyloxy-6-methoxy-4-methoxycarbonylphenyl ketone

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Technology Process of 2-benzyloxy-6-methoxycarbonylphenyl 2-benzyloxy-6-methoxy-4-methoxycarbonylphenyl ketone

There total 5 articles about 2-benzyloxy-6-methoxycarbonylphenyl 2-benzyloxy-6-methoxy-4-methoxycarbonylphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 100-39-0
benzyl bromide

: 171009-51-1
2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone

: 171009-39-5
2-benzyloxy-6-methoxycarbonylphenyl 2-benzyloxy-6-methoxy-4-methoxycarbonylphenyl ketone

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 65 ℃; for 2h;

Reference yield:

: 38197-43-2
2-bromo-3-methylanisole

: 171009-39-5
2-benzyloxy-6-methoxycarbonylphenyl 2-benzyloxy-6-methoxy-4-methoxycarbonylphenyl ketone

Guidance literature:: Multi-step reaction with 6 steps

1: 1) Mg, 1,2-dibromoethane / 1) THF, reflux, 1 h, 2) room temperature, 30 min

2: 38 percent / KMnO₄, NaOH / methanol; pyridine / Heating

3: SOCl₂ / 2 h / Heating

4: 0.9 g / BBr₃ / CH₂Cl₂ / 18 h / -60 deg C -> room temperature

5: 100 percent / SOCl₂ / 3 h / Heating

6: 74 percent / NaH / dimethylformamide / 2 h / 65 °C

With sodium hydroxide; potassium permanganate; thionyl chloride; boron tribromide; sodium hydride; magnesium; ethylene dibromide; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 54812-40-7
2,6-dimethoxy-4-methylbenzoyl chloride

: 171009-39-5
2-benzyloxy-6-methoxycarbonylphenyl 2-benzyloxy-6-methoxy-4-methoxycarbonylphenyl ketone

Guidance literature:: Multi-step reaction with 6 steps

1: 1) Mg, 1,2-dibromoethane / 1) THF, reflux, 1 h, 2) room temperature, 30 min

2: 38 percent / KMnO₄, NaOH / methanol; pyridine / Heating

3: SOCl₂ / 2 h / Heating

4: 0.9 g / BBr₃ / CH₂Cl₂ / 18 h / -60 deg C -> room temperature

5: 100 percent / SOCl₂ / 3 h / Heating

6: 74 percent / NaH / dimethylformamide / 2 h / 65 °C

With sodium hydroxide; potassium permanganate; thionyl chloride; boron tribromide; sodium hydride; magnesium; ethylene dibromide; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;