2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone

Base Information

Chemical Name:2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone
CAS No.:171009-51-1
Molecular Formula:C₁₈H₁₆O₈
Molecular Weight:360.32
Hs Code.:

Synonyms:2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone

Suppliers and Price of 2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone

There total 5 articles about 2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 171009-38-4
4-carboxy-2-hydroxy-6-methoxyphenyl 2-carboxy-6-hydroxyphenyl ketone

: 171009-51-1
2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone

Guidance literature:: With thionyl chloride; for 3h; Heating;

Reference yield:

: 38197-43-2
2-bromo-3-methylanisole

: 171009-51-1
2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Mg, 1,2-dibromoethane / 1) THF, reflux, 1 h, 2) room temperature, 30 min

2: 38 percent / KMnO₄, NaOH / methanol; pyridine / Heating

3: SOCl₂ / 2 h / Heating

4: 0.9 g / BBr₃ / CH₂Cl₂ / 18 h / -60 deg C -> room temperature

5: 100 percent / SOCl₂ / 3 h / Heating

With sodium hydroxide; potassium permanganate; thionyl chloride; boron tribromide; magnesium; ethylene dibromide; In pyridine; methanol; dichloromethane;

Reference yield:

: 54812-40-7
2,6-dimethoxy-4-methylbenzoyl chloride

: 171009-51-1
2-hydroxy-6-methoxycarbonylphenyl 2-hydroxy-6-methoxy-4-methoxycarbonylphenyl ketone

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Mg, 1,2-dibromoethane / 1) THF, reflux, 1 h, 2) room temperature, 30 min

2: 38 percent / KMnO₄, NaOH / methanol; pyridine / Heating

3: SOCl₂ / 2 h / Heating

4: 0.9 g / BBr₃ / CH₂Cl₂ / 18 h / -60 deg C -> room temperature

5: 100 percent / SOCl₂ / 3 h / Heating

With sodium hydroxide; potassium permanganate; thionyl chloride; boron tribromide; magnesium; ethylene dibromide; In pyridine; methanol; dichloromethane;