2-n-hexyloxy-5-nitrobenzonitrile

Base Information

Chemical Name:2-n-hexyloxy-5-nitrobenzonitrile
CAS No.:288252-01-7
Molecular Formula:C₁₃H₁₆N₂O₃
Molecular Weight:248.282
Hs Code.:

Synonyms:2-n-hexyloxy-5-nitrobenzonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-n-hexyloxy-5-nitrobenzonitrile

Chemical Property:

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Technology Process of 2-n-hexyloxy-5-nitrobenzonitrile

There total 5 articles about 2-n-hexyloxy-5-nitrobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 611-20-1
salicylonitrile

: 288252-01-7
2-n-hexyloxy-5-nitrobenzonitrile

Guidance literature:: salicylonitrile; With nitric acid; acetic acid; at 50 - 70 ℃; for 4h;

n-hexyl halide; With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1016/j.bmcl.2017.06.059

Reference yield:

: 16588-15-1
2-chloro-5-nitro-benzamide

: 288252-01-7
2-n-hexyloxy-5-nitrobenzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: benzenesulfonyl chloride / DMF (N,N-dimethyl-formamide); toluene / 3 h / 20 - 145 °C

2: sodium hydride / DMF (N,N-dimethyl-formamide) / 1 h / Ice cooling

With sodium hydride; benzenesulfonyl chloride; In DMF (N,N-dimethyl-formamide); toluene;

Reference yield:

: 2516-96-3
2-chloro-5-nitrobenzoic acid

: 288252-01-7
2-n-hexyloxy-5-nitrobenzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / DMF (N,N-dimethyl-formamide); toluene / 3 h / 20 °C / Heating / reflux

1.2: Ice cooling

2.1: benzenesulfonyl chloride / DMF (N,N-dimethyl-formamide); toluene / 3 h / 20 - 145 °C

3.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1 h / Ice cooling

With thionyl chloride; sodium hydride; benzenesulfonyl chloride; In DMF (N,N-dimethyl-formamide); toluene;