Acetate, 2-bromo-,2,2,2-trichloroethyl ester

Base Information

• Chemical Name: Acetate, 2-bromo-,2,2,2-trichloroethyl ester
• CAS No.: 55110-70-8
• Molecular Formula: C4H4BrCl3O2
• Molecular Weight: 270.338
• Hs Code.: 2915900090
• Mol file: 55110-70-8.mol

Synonyms:Acetate, 2-bromo-,2,2,2-trichloroethyl ester

Chemical Property of Acetate, 2-bromo-,2,2,2-trichloroethyl ester

Chemical Property:

• Vapor Pressure: 0.00066mmHg at 25°C
• Boiling Point: 308.9°C at 760 mmHg
• Flash Point: 140.6°C
• PSA: 26.30000
• Density: 1.858g/cm³
• LogP: 2.29470

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetate, 2-bromo-,2,2,2-trichloroethyl ester

There total 1 articles about Acetate, 2-bromo-,2,2,2-trichloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromoacetyl chloride (22118-09-8) + 1,1,1-trichloroethanol (115-20-8) → 2,2,2-trichloroethyl 2-bromoacetate (55110-70-8)

Guidance literature:

In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/jm020526p

Reference yield: 80.0%

2,2,2-trichloroethyl 2-bromoacetate (55110-70-8) + allyl 5-hydroxy-2-{[(S)-2-(hydroxymethyl)pyrrolidinyl]carbonyl}-4-methoxyphenylcarbamate (550355-92-5) → 2,2,2-trichloroethyl (5-{[(allyloxy)carbonyl]amino}-4-{[(2S)-2-(hydroxymethyl)pyrrolidinyl]carbonyl}-2-methoxyphenoxy)acetate (550355-94-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1021/jm020526p

Reference yield:

2-bromo-2-methylpropionic acid methyl ester (23426-63-3) + methyl 2-iodoacetate (5199-50-8) + Methyl 2-bromopropionate (5445-17-0) + 2,2,2-trichloroethyl 2-bromoacetate (55110-70-8) + methyl chloroacetate (96-34-4) → 2,2-dimethylbutyric acid (595-37-9)

Guidance literature:

In 2,2,2-trichloroethyl butyrate;

upstream raw materials:

2-bromoacetyl chloride

1,1,1-trichloroethanol

Downstream raw materials:

2,2,2-trichloroethyl (5-{[(allyloxy)carbonyl]amino}-4-{[(2S)-2-(hydroxymethyl)pyrrolidinyl]carbonyl}-2-methoxyphenoxy)acetate

2,2-dimethylbutyric acid

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