4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate

Base Information

Chemical Name:4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate
CAS No.:1354789-15-3
Molecular Formula:C₂₄H₂₈BFeNO₄
Molecular Weight:461.149
Hs Code.:

Synonyms:4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate

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Chemical Property of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate

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Technology Process of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate

There total 2 articles about 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: ferrocenoyl azide

: 302348-51-2
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

: 1354789-15-3
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate

Guidance literature:: In toluene; for 2h; Inert atmosphere; Reflux;
DOI:10.1039/c7ob00211d

Reference yield:

: 1273-82-1
aminoferrocene

: 32315-10-9
bis(trichloromethyl) carbonate

: 302348-51-2
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

: 1354789-15-3
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate

Guidance literature:: at 120 ℃; for 24h;
DOI:10.1021/jm5019548

Reference yield: 92.0%

: 1354789-15-3
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate

: 100-39-0
benzyl bromide

: 1354789-19-7
4-[(N-benzyl-N-ferrocenylaminocarbonyl)oxymethyl]-2-phenylboronic acid pinacol ester

Guidance literature:: 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl ferrocenylcarbamate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 22 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; Inert atmosphere;
DOI:10.1021/jm5019548