4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol

Base Information

• Chemical Name: 4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol
• CAS No.: 503622-16-0
• Molecular Formula: C₇₃H₁₀₄O₄Si₃
• Molecular Weight: 1129.88

Synonyms:4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol

Chemical Property of 4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol

There total 3 articles about 4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4-triallylmethylphenol (224191-80-4) + propionic acid 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenyl ester (503622-15-9) → 4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol (503622-16-0)

Guidance literature:

4-triallylmethylphenol; propionic acid 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenyl ester; With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 48h;

With water; potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 24h; Further stages.;

DOI:10.1039/b210358n

Reference yield:

4-triallylmethylphenol (224191-80-4) → 4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol (503622-16-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 91 percent / diethyl ether / 48 h / 20 °C

2.1: 99 percent / NaI / butan-2-one / 24 h / 80 °C

3.1: 91 percent / NEt(iPr)2 / CH₂Cl₂ / 16 h / 20 °C

4.1: K₂CO₃ / dimethylformamide / 48 h / 80 °C

4.2: 68 percent / H₂O; K₂CO₃ / dimethylformamide / 24 h / 80 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; butanone;

DOI:10.1039/b210358n

Reference yield:

4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol (527698-54-0) → 4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol (503622-16-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 91 percent / NEt(iPr)2 / CH₂Cl₂ / 16 h / 20 °C

2.1: K₂CO₃ / dimethylformamide / 48 h / 80 °C

2.2: 68 percent / H₂O; K₂CO₃ / dimethylformamide / 24 h / 80 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/b210358n

upstream raw materials:

4-triallylmethylphenol

propionic acid 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenyl ester

4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 503622-16-0 4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol

Send

Send

Metric Ton KG G Pound L ML

Send

Send