4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol

Base Information

• Chemical Name: 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol
• CAS No.: 527698-54-0
• Molecular Formula: C₂₅H₄₇I₃OSi₃
• Molecular Weight: 828.618

Synonyms:4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol

Chemical Property of 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol

Chemical Property:

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Technology Process of 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol

There total 2 articles about 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-{4-(chloromethyl-dimethyl-silanyl)-1,1-bis-[3-(chloromethyl-dimethyl-silanyl)-propyl]-butyl}-phenol (387339-00-6) → 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol (527698-54-0)

Guidance literature:

With sodium iodide; In butanone; at 80 ℃; for 24h;

DOI:10.1039/b210358n

Reference yield:

4-triallylmethylphenol (224191-80-4) → 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol (527698-54-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / diethyl ether / 48 h / 20 °C

2: 99 percent / NaI / butan-2-one / 24 h / 80 °C

With sodium iodide; In diethyl ether; butanone;

DOI:10.1039/b210358n

Reference yield: 91.0%

ethyl iodoacetate (598-40-3) + 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenol (527698-54-0) → propionic acid 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenyl ester (503622-15-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1039/b210358n

upstream raw materials:

4-{4-(chloromethyl-dimethyl-silanyl)-1,1-bis-[3-(chloromethyl-dimethyl-silanyl)-propyl]-butyl}-phenol

4-triallylmethylphenol

Downstream raw materials:

propionic acid 4-{4-(iodomethyl-dimethyl-silanyl)-1,1-bis-[3-(iodomethyl-dimethyl-silanyl)-propyl]-butyl}-phenyl ester

4-[4-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-1,1-bis-(3-{[4-(1,1-diallyl-but-3-enyl)-phenoxymethyl]-dimethyl-silanyl}-propyl)-butyl]-phenol

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