4-(4-METHOXY-PHENYL)-1,4-DIHYDRO-BENZO[4,5]IMIDAZO[1,2-A][1,3,5]TRIAZIN-2-YLAMINE

Base Information

• Chemical Name: 4-(4-METHOXY-PHENYL)-1,4-DIHYDRO-BENZO[4,5]IMIDAZO[1,2-A][1,3,5]TRIAZIN-2-YLAMINE
• CAS No.: 78650-03-0
• Molecular Formula: C₁₆H₁₅N₅O
• Molecular Weight: 293.328
• Mol file: 78650-03-0.mol

Synonyms:4-(4-methoxyphenyl)-3,4-dihydro[1,3,5]triazino[1,2-a]benzimidazole-2-amine

Chemical Property of 4-(4-METHOXY-PHENYL)-1,4-DIHYDRO-BENZO[4,5]IMIDAZO[1,2-A][1,3,5]TRIAZIN-2-YLAMINE

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

4-(4-Methoxyphenyl)-1,4-dihydro[1,3,5]triazino-[1,2-a]benzimidazol-2-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4-(4-METHOXY-PHENYL)-1,4-DIHYDRO-BENZO[4,5]IMIDAZO[1,2-A][1,3,5]TRIAZIN-2-YLAMINE

There total 2 articles about 4-(4-METHOXY-PHENYL)-1,4-DIHYDRO-BENZO[4,5]IMIDAZO[1,2-A][1,3,5]TRIAZIN-2-YLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-guanidinobenzimidazole (5418-95-1) + 4-methoxy-benzaldehyde (123-11-5) → 4-(4-methoxyphenyl)-3,4-dihydro[1,3,5]triazino[1,2-a]benzimidazole-2-amine (78650-03-0)

Guidance literature:

With piperidine; In ethanol; Heating;

DOI:10.1002/jhet.5570430614

Reference yield:

1,2-diamino-benzene (95-54-5) → 4-(4-methoxyphenyl)-3,4-dihydro[1,3,5]triazino[1,2-a]benzimidazole-2-amine (78650-03-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Reflux; Acidic conditions

2: piperidine / ethanol / Reflux

With piperidine; In ethanol;

DOI:10.13005/ojc/310213

Reference yield: 81.0%

ethyl acetoacetate (141-97-9) + 4-(4-methoxyphenyl)-3,4-dihydro[1,3,5]triazino[1,2-a]benzimidazole-2-amine (78650-03-0) → 6-(4-methoxyphenyl)-4-methyl-6H-benzo[4,5]imidazo[1,2-a]pyrimido[2,1-d][1,3,5]triazin-2(1H)-one

Guidance literature:

In N,N-dimethyl-formamide; for 6h; Reflux;

DOI:10.13005/ojc/310213

upstream raw materials:

2-guanidinobenzimidazole

4-methoxy-benzaldehyde

1,2-diamino-benzene

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