1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate

Base Information

Chemical Name:1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate
CAS No.:937811-11-5
Molecular Formula:C₃₁H₃₉NO₅
Molecular Weight:505.654
Hs Code.:

Synonyms:1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate

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Chemical Property of 1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate

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Technology Process of 1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate

There total 10 articles about 1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: π-(β-cyclolavandulyl)nickel bromide

: 197504-73-7
1-[6-bromo-3,4-dimethoxy-2-methyl-(9H-carbazol-1-yl)]propan-2-yl acetate

: 1378348-36-7
1,2-bis-(2,4,4-trimethyl-1-cyclohexen-1-yl)ethane

: 937811-11-5
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate

: 207505-90-6
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.3998/ark.5550190.0013.323

Reference yield:

: 18088-97-6
(2,4,4-trimethyl-1-cyclohexen-1-yl)carboxylic acid

: 937811-11-5
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate

: 207505-90-6
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 3.25 h / 0 °C / Inert atmosphere

2: phosphorus tribromide; pyridine / diethyl ether / 1.5 h / -78 - 20 °C / Inert atmosphere

3: benzene / 2.5 h / 60 - 65 °C / Inert atmosphere

4: N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; phosphorus tribromide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; benzene;
DOI:10.3998/ark.5550190.0013.323

Reference yield:

: 103985-40-6
(2,4,4-trimethyl-1-cyclohexen-1-yl)methanol

: 937811-11-5
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate

: 207505-90-6
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide; pyridine / diethyl ether / 1.5 h / -78 - 20 °C / Inert atmosphere

2: benzene / 2.5 h / 60 - 65 °C / Inert atmosphere

3: N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

With pyridine; phosphorus tribromide; In diethyl ether; N,N-dimethyl-formamide; benzene;
DOI:10.3998/ark.5550190.0013.323