(4S,5S)-N4,N5,2,2-tetramethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanamine

Base Information

Chemical Name:(4S,5S)-N4,N5,2,2-tetramethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanamine
CAS No.:147700-76-3
Molecular Formula:C₃₃H₃₆N₂O₂
Molecular Weight:492.661
Hs Code.:

Synonyms:(4S,5S)-N4,N5,2,2-tetramethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanamine

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Chemical Property of (4S,5S)-N4,N5,2,2-tetramethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanamine

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Technology Process of (4S,5S)-N4,N5,2,2-tetramethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanamine

There total 7 articles about (4S,5S)-N4,N5,2,2-tetramethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2,2-dimethyl N,N-diformyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-di(methylamine)

: 147700-76-3
(4S,5S)-N4,N5,2,2-tetramethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanamine

Guidance literature:: With lithium aluminium tetrahydride; In 1,2-dimethoxyethane; for 12h; Heating;
DOI:10.1055/s-1993-26041

Reference yield: 62.0%

: 147700-73-0
(4R,5R)-4,5-bis[chloro(diphenyl)methyl]-2,2-dimethyl-1,3-dioxolane

: 74-89-5
methylamine

: 1399829-62-9
(3S,4S)-1-methyl-2,2,5,5-tetraphenylpyrrolidine-3,4-diol

: 1399829-60-7
(3aS,6aS)-tetrahydro-2,2,5-trimethyl-4,4,6,6-tetraphenyl-4H-1,3-dioxolo[4,5-c]pyrrole

: 147700-76-3
(4S,5S)-N4,N5,2,2-tetramethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanamine

Guidance literature:: (4R,5R)-4,5-bis[chloro(diphenyl)methyl]-2,2-dimethyl-1,3-dioxolane; methylamine; With ammonium chloride; at 100 ℃; for 48h; under 22502.3 Torr; Autoclave; Inert atmosphere;

With water; silica gel;
DOI:10.1002/hlca.201200147