Technology Process of C31H53NO5
There total 5 articles about C31H53NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
ethanol;
at 20 ℃;
for 27h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dihydrogen peroxide; sulfuric acid / methanol / 2 h / 20 °C / Inert atmosphere; Reflux
2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere
2.2: 13 h / 20 °C
3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; hexane / 2.08 h / -78 - 0 °C
3.2: 15 h / 20 °C
4.1: ammonium cerium (IV) nitrate / acetonitrile / 3.5 h / -7 - 20 °C
5.1: sodium hydrogencarbonate / ethanol / 27 h / 20 °C
With
n-butyllithium; ammonium cerium (IV) nitrate; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; dihydrogen peroxide; sodium hydride; sodium hydrogencarbonate;
In
tetrahydrofuran; methanol; ethanol; hexane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; hexane / 2.08 h / -78 - 0 °C
1.2: 15 h / 20 °C
2.1: ammonium cerium (IV) nitrate / acetonitrile / 3.5 h / -7 - 20 °C
3.1: sodium hydrogencarbonate / ethanol / 27 h / 20 °C
With
n-butyllithium; ammonium cerium (IV) nitrate; N,N,N,N,-tetramethylethylenediamine; sodium hydrogencarbonate;
In
tetrahydrofuran; ethanol; hexane; acetonitrile;