α-(diphenylmethylamino)-2-methylbenzeneacetic acid

Base Information

Chemical Name:α-(diphenylmethylamino)-2-methylbenzeneacetic acid
CAS No.:1194752-71-0
Molecular Formula:C₂₂H₂₁NO₂
Molecular Weight:331.414
Hs Code.:

Synonyms:α-(diphenylmethylamino)-2-methylbenzeneacetic acid

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Chemical Property of α-(diphenylmethylamino)-2-methylbenzeneacetic acid

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Technology Process of α-(diphenylmethylamino)-2-methylbenzeneacetic acid

There total 1 articles about α-(diphenylmethylamino)-2-methylbenzeneacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 16419-60-6
2-Methylphenylboronic acid

: 298-12-4
Glyoxilic acid

: 91-00-9
Benzhydrylamine

: 1194752-71-0
α-(diphenylmethylamino)-2-methylbenzeneacetic acid

Guidance literature:: 2-Methylphenylboronic acid; Glyoxilic acid; Benzhydrylamine; In dichloromethane; at 20 ℃; for 150.25h; Inert atmosphere;

In water; Reflux;

Reference yield: 45.0%

: 1194752-71-0
α-(diphenylmethylamino)-2-methylbenzeneacetic acid

: 1194752-74-3
α-(diphenylmethylamino)-2-methylbenzeneacetamide

Guidance literature:: α-(diphenylmethylamino)-2-methylbenzeneacetic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

With ammonium chloride; In N,N-dimethyl-formamide; at 20 ℃; for 138h;

Reference yield:

: 1194752-71-0
α-(diphenylmethylamino)-2-methylbenzeneacetic acid

: 203065-98-9
(+/-)-2-methylphenylglycine amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

1.2: 138 h / 20 °C

2.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / methanol; water / 5 h / 2585.81 Torr

With hydrogenchloride; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In methanol; water; N,N-dimethyl-formamide;