N-[6-Amino-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)-propoxy}]phenyl-N'-pentylurea

Base Information

Chemical Name:N-[6-Amino-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)-propoxy}]phenyl-N'-pentylurea
CAS No.:141815-90-9
Molecular Formula:C₂₅H₃₃N₅O₂
Molecular Weight:435.569
Hs Code.:

Synonyms:N-[6-Amino-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)-propoxy}]phenyl-N'-pentylurea

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Chemical Property of N-[6-Amino-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)-propoxy}]phenyl-N'-pentylurea

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Technology Process of N-[6-Amino-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)-propoxy}]phenyl-N'-pentylurea

There total 6 articles about N-[6-Amino-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)-propoxy}]phenyl-N'-pentylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 141799-80-6
N-[6-nitro-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propoxy}]phenyl-N'-pentylurea

: 141815-90-9
N-[6-Amino-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)-propoxy}]phenyl-N'-pentylurea

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; under 3677.5 Torr;
DOI:10.1021/jm00063a014

Reference yield:

: 144-55-8
sodium hydrogencarbonate

: 141799-80-6
N-[6-nitro-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propoxy}]phenyl-N'-pentylurea

: 141815-90-9
N-[6-Amino-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)-propoxy}]phenyl-N'-pentylurea

Guidance literature:: palladium-carbon; In ethanol; hydrogen; acetic acid;

Reference yield:

: 603-85-0
2-Amino-3-nitrophenol

: 141815-90-9
N-[6-Amino-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl)-propoxy}]phenyl-N'-pentylurea

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / NaI, K₂CO₃ / dimethylformamide / 2 h / 60 °C

2: 70 percent / pyridine / 3 h / 100 °C

3: 44 percent / toluene / 1 h / Heating

4: 83 percent / H₂ / Pd/C / acetic acid / 3677.5 Torr

With pyridine; hydrogen; potassium carbonate; sodium iodide; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00063a014