(octaethylporphyrin)Fe(p-MeC₆H₄)

Base Information

Chemical Name:(octaethylporphyrin)Fe(p-MeC₆H₄)
CAS No.:83614-08-8
Molecular Formula:C₄₃H₅₁FeN₄
Molecular Weight:679.752
Hs Code.:

(octaethylporphyrin)Fe(p-MeC<sub>6</sub>H<sub>4</sub>)

Synonyms:(octaethylporphyrin)Fe(p-MeC₆H₄)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (octaethylporphyrin)Fe(p-MeC₆H₄)

Chemical Property:

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Technology Process of (octaethylporphyrin)Fe(p-MeC₆H₄)

There total 2 articles about (octaethylporphyrin)Fe(p-MeC₆H₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 50540-30-2
{(octaethylporphyrin)FeClO₄}⁽¹⁺⁾

: 4294-57-9
para-methylphenylmagnesium bromide

: 83614-08-8
(octaethylporphyrin)Fe(p-MeC₆H₄)

Guidance literature:: In diethyl ether; benzene; complex stirred in C6H6, org. educt soln. in ether added, stirred for 1h at room temp.; concd. (vac.), chromd. (SiO2, C6H6), evapd. (vac.), recrystd. (C6H6/petroleum ether); elem. anal.;
DOI:10.1016/S0022-328X(00)85854-4

Reference yield: 43.0%

: 28755-93-3
iron(III)octaethylporphyrin chloride

: 696-61-7
4-tolylmagnesium chloride

: 83614-08-8
(octaethylporphyrin)Fe(p-MeC₆H₄)

Guidance literature:: In benzene; 1 equiv of benzene soln. of p-TolMgCl was added dropwise under vigorousstirring at 5-6°C under inert atmosphere to a soln. of Fe-complex in benzene, the mixt. was stirred for several min; carefully hydrolyzed with Ar-satd. water, org. phase was sepd., washed until it became neutral, dried over MgSO4, evapd. in vacuo below 40°C, residue was chromd. over Al2O3 (eluent benzene) in the dark, recrystd. from C6H6-pentane; elem. anal.;
DOI:10.1016/0022-328X(83)80109-0

Reference yield:

: 83614-08-8
(octaethylporphyrin)Fe(p-MeC₆H₄)

: 28755-93-3
iron(III)octaethylporphyrin chloride

: 100-66-3
methoxybenzene

Guidance literature:: With HCl; H₂O; In tetrahydrofuran; water; aq. HCl added to complex soln. in THF; ppt. crystd. (CH2Cl2/petroleum ether), obtained as mixt.;
DOI:10.1016/S0022-328X(00)85854-4