3,4,6-tri-O-acetyl-2-C:1-N-carbonyl-2-deoxy-N-(p-tolylsulfonyl)-α-D-glucopyranosylamine

Base Information

Chemical Name:3,4,6-tri-O-acetyl-2-C:1-N-carbonyl-2-deoxy-N-(p-tolylsulfonyl)-α-D-glucopyranosylamine
CAS No.:95068-98-7
Molecular Formula:C₂₀H₂₃NO₁₀S
Molecular Weight:469.469
Hs Code.:

Synonyms:3,4,6-tri-O-acetyl-2-C:1-N-carbonyl-2-deoxy-N-(p-tolylsulfonyl)-α-D-glucopyranosylamine

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Chemical Property of 3,4,6-tri-O-acetyl-2-C:1-N-carbonyl-2-deoxy-N-(p-tolylsulfonyl)-α-D-glucopyranosylamine

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Technology Process of 3,4,6-tri-O-acetyl-2-C:1-N-carbonyl-2-deoxy-N-(p-tolylsulfonyl)-α-D-glucopyranosylamine

There total 1 articles about 3,4,6-tri-O-acetyl-2-C:1-N-carbonyl-2-deoxy-N-(p-tolylsulfonyl)-α-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 4083-64-1
Tosyl isocyanate

: 2873-29-2
D-glucal triacetate

: 95068-98-7
3,4,6-tri-O-acetyl-2-C:1-N-carbonyl-2-deoxy-N-(p-tolylsulfonyl)-α-D-glucopyranosylamine

Guidance literature:: In diethyl ether; for 20h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96639-6

Reference yield: 70.0%

: 67-56-1
methanol

: 95068-98-7
3,4,6-tri-O-acetyl-2-C:1-N-carbonyl-2-deoxy-N-(p-tolylsulfonyl)-α-D-glucopyranosylamine

: 95069-01-5
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-6-methoxy-5-(toluene-4-sulfonylaminocarbonyl)-tetrahydro-pyran-4-yl ester

Guidance literature:: for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96639-6

Reference yield:

: 95068-98-7
3,4,6-tri-O-acetyl-2-C:1-N-carbonyl-2-deoxy-N-(p-tolylsulfonyl)-α-D-glucopyranosylamine

: 2873-29-2
D-glucal triacetate

Guidance literature:: In chloroform-d1; at 20 ℃; under 760 Torr; time course of the retroaddition, other solvent, other temperature, other substrates;