Asparic acid 2-hydroxyethylthioethyl ester

Base Information

Chemical Name:Asparic acid 2-hydroxyethylthioethyl ester
CAS No.:186534-36-1
Molecular Formula:C₈H₁₅NO₅S
Molecular Weight:237.277
Hs Code.:

Synonyms:Asparic acid 2-hydroxyethylthioethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Asparic acid 2-hydroxyethylthioethyl ester

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Technology Process of Asparic acid 2-hydroxyethylthioethyl ester

There total 1 articles about Asparic acid 2-hydroxyethylthioethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1122-58-3
dmap

: 111-48-8
2,2'-thiobis-ethanol

: 34582-32-6
N-tert-butoxycarbonyl aspartic acid tert-butyl ester

: 538-75-0
dicyclohexyl-carbodiimide

: 76-05-1
trifluoroacetic acid

: 2-tert-butoxycarbonylamino-succinic acid 1-tert-butyl ester 4-[2-(2-hydroxy-ethylsulfanyl)-ethyl] ester

: 2387-23-7
1,3-Dicyclohexylurea

: 186534-36-1
Asparic acid 2-hydroxyethylthioethyl ester

Guidance literature:: dmap; 2,2'-thiobis-ethanol; N-tert-butoxycarbonyl aspartic acid tert-butyl ester; dicyclohexyl-carbodiimide; In ethyl acetate; at 0 - 20 ℃; for 16h;

trifluoroacetic acid; 2-tert-butoxycarbonylamino-succinic acid 1-tert-butyl ester 4-[2-(2-hydroxy-ethylsulfanyl)-ethyl] ester; In trifluoroacetic acid; at 20 ℃; for 5h;
DOI:10.1007/s002040050372