phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-methanesulfonyloxyethyl)diamidophosphoric acid

Base Information

Chemical Name:phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-methanesulfonyloxyethyl)diamidophosphoric acid
CAS No.:81175-81-7
Molecular Formula:C₁₆H₂₇Cl₂N₂O₈PS₂
Molecular Weight:541.411
Hs Code.:

Synonyms:phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-methanesulfonyloxyethyl)diamidophosphoric acid

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Chemical Property of phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-methanesulfonyloxyethyl)diamidophosphoric acid

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Technology Process of phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-methanesulfonyloxyethyl)diamidophosphoric acid

There total 3 articles about phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-methanesulfonyloxyethyl)diamidophosphoric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 124-63-0
methanesulfonyl chloride

: 81175-73-7
phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-hydroxyethyl)diamidophosphoric acid

: 81175-81-7
phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-methanesulfonyloxyethyl)diamidophosphoric acid

Guidance literature:: With triethylamine; In acetone; 1) 0 to 10 deg C, , 2) 0 deg C, 1 h;

Reference yield:

: 4798-75-8
phenyl N,N-bis(2-chloroethyl)phosphoramidochloridate

: 81175-81-7
phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-methanesulfonyloxyethyl)diamidophosphoric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Et₃N / acetone / 1) heating, 15 h, 2) 0 to 5 deg C,

2: 94 percent / Et₃N / acetone / 1) 0 to 10 deg C, , 2) 0 deg C, 1 h

With triethylamine; In acetone;

Reference yield:

: 108-95-2,27073-41-2
phenol

: 81175-81-7
phenyl ester of N,N-bis(2-chloroethyl)-N',N'-bis(2-methanesulfonyloxyethyl)diamidophosphoric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / Et₃N / benzene / 1) heating, 3 h, 2) r.t.,

2: 93 percent / Et₃N / acetone / 1) heating, 15 h, 2) 0 to 5 deg C,

3: 94 percent / Et₃N / acetone / 1) 0 to 10 deg C, , 2) 0 deg C, 1 h

With triethylamine; In acetone; benzene;