4-[2-(2,2,2-Trifluoro-acetylamino)-ethoxy]-benzimidic acid methyl ester

Base Information

Chemical Name:4-[2-(2,2,2-Trifluoro-acetylamino)-ethoxy]-benzimidic acid methyl ester
CAS No.:179749-10-1
Molecular Formula:C₁₂H₁₃F₃N₂O₃
Molecular Weight:290.242
Hs Code.:

Synonyms:4-[2-(2,2,2-Trifluoro-acetylamino)-ethoxy]-benzimidic acid methyl ester

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Chemical Property of 4-[2-(2,2,2-Trifluoro-acetylamino)-ethoxy]-benzimidic acid methyl ester

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Technology Process of 4-[2-(2,2,2-Trifluoro-acetylamino)-ethoxy]-benzimidic acid methyl ester

There total 1 articles about 4-[2-(2,2,2-Trifluoro-acetylamino)-ethoxy]-benzimidic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67-56-1
methanol

: N-[2-(4-Cyano-phenoxy)-ethyl]-2,2,2-trifluoro-acetamide

: 179749-10-1
4-[2-(2,2,2-Trifluoro-acetylamino)-ethoxy]-benzimidic acid methyl ester

Guidance literature:: With hydrogenchloride; In dichloromethane; for 0h;
DOI:10.1021/ja960948m

Reference yield: 45.0%

: 179749-10-1
4-[2-(2,2,2-Trifluoro-acetylamino)-ethoxy]-benzimidic acid methyl ester

: 23491-49-8
2-amino-4-<5'-(4''-methylpiperazin-1''-yl)benzimidazol-2'-yl>aniline

: 179749-11-2
2,2,2-Trifluoro-N-(2-{4-[5-(4-methyl-piperazin-1-yl)-1H,1'H-[2,5']bibenzoimidazolyl-2'-yl]-phenoxy}-ethyl)-acetamide

Guidance literature:: With acetic acid; In methanol; at 65 - 70 ℃; for 3h; Heating;
DOI:10.1021/ja960948m

Reference yield:

: 179749-10-1
4-[2-(2,2,2-Trifluoro-acetylamino)-ethoxy]-benzimidic acid methyl ester

: 179749-12-3
2-{4-[5-(4-Methyl-piperazin-1-yl)-1H,1'H-[2,5']bibenzoimidazolyl-2'-yl]-phenoxy}-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / AcOH / methanol / 3 h / 65 - 70 °C / Heating

2: 94 percent / aq. K₂CO₃ / methanol / Ambient temperature

With potassium carbonate; acetic acid; In methanol;
DOI:10.1021/ja960948m