2-[3-(diethoxyphosphorylmethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)-pyridine

Base Information

Chemical Name:2-[3-(diethoxyphosphorylmethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)-pyridine
CAS No.:1428929-31-0
Molecular Formula:C₁₈H₂₁F₃NO₄P
Molecular Weight:403.338
Hs Code.:

Synonyms:2-[3-(diethoxyphosphorylmethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)-pyridine

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Chemical Property of 2-[3-(diethoxyphosphorylmethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)-pyridine

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Technology Process of 2-[3-(diethoxyphosphorylmethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)-pyridine

There total 7 articles about 2-[3-(diethoxyphosphorylmethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428929-30-9
2-[3-(chloromethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)pyridine

: 122-52-1
triethyl phosphite

: 1428929-31-0
2-[3-(diethoxyphosphorylmethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)-pyridine

Guidance literature:: at 130 ℃; for 18h;

Reference yield:

: 52334-81-3
2-chloro-5-trifluoromethylpyridine

: 1428929-31-0
2-[3-(diethoxyphosphorylmethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)-pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 100 °C

2: thionyl chloride / dichloromethane / 1 h / 0 - 20 °C

3: 18 h / 130 °C

With thionyl chloride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1428929-79-6
ethoxycarbonyl 3-ethoxycarbonyloxy-5-methyl-benzoate

: 1428929-31-0
2-[3-(diethoxyphosphorylmethyl)-5-methyl-phenoxy]-5-(trifluoromethyl)-pyridine

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C

2: sodium hydroxide / ethanol; water / 1 h / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 2 h / 100 °C

4: thionyl chloride / dichloromethane / 1 h / 0 - 20 °C

5: 18 h / 130 °C

With sodium tetrahydroborate; thionyl chloride; potassium carbonate; sodium hydroxide; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;