C₆₄H₇₈N₈O₁₀S₄

Base Information

Chemical Name:C₆₄H₇₈N₈O₁₀S₄
CAS No.:170862-04-1
Molecular Formula:C₆₄H₇₈N₈O₁₀S₄
Molecular Weight:1247.63
Hs Code.:

C<sub>64</sub>H<sub>78</sub>N<sub>8</sub>O<sub>10</sub>S<sub>4</sub>

Synonyms:C₆₄H₇₈N₈O₁₀S₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₄H₇₈N₈O₁₀S₄

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Technology Process of C₆₄H₇₈N₈O₁₀S₄

There total 12 articles about C₆₄H₇₈N₈O₁₀S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111-94-4
3,3'-Iminodipropionitrile

: 170862-04-1
C₆₄H₇₈N₈O₁₀S₄

Guidance literature:: Multi-step reaction with 6 steps

1: 64 percent / Et₃N / CH₂Cl₂ / 20 °C

2: 92 percent / H₂, NH₃ / Raney nickel / methanol / 48 h / 20 °C / 2327.17 Torr

3: 43 percent / Et₃N / CH₂Cl₂ / 20 °C

4: Cs₂CO₃ / dimethylformamide / 24 h / 65 °C

5: glac. AcOH, HBr / 2 h / 20 °C

6: K₂CO₃ / acetonitrile / 22 h / Heating

With ammonia; hydrogen bromide; hydrogen; potassium carbonate; caesium carbonate; acetic acid; triethylamine; nickel; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: protection of the amino group / 2: Hydrogenation / 3: Tosylation / 4: cyclocondensation / 5: diethoxyphosphoryl deprotection / 6: Condensation;
DOI:10.1021/jm990211i

Reference yield:

: 90974-12-2
N-diethoxyphosphoryl-3,3'-iminodipropionitrile

: 170862-04-1
C₆₄H₇₈N₈O₁₀S₄

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / H₂, NH₃ / Raney nickel / methanol / 48 h / 20 °C / 2327.17 Torr

2: 43 percent / Et₃N / CH₂Cl₂ / 20 °C

3: Cs₂CO₃ / dimethylformamide / 24 h / 65 °C

4: glac. AcOH, HBr / 2 h / 20 °C

5: K₂CO₃ / acetonitrile / 22 h / Heating

With ammonia; hydrogen bromide; hydrogen; potassium carbonate; caesium carbonate; acetic acid; triethylamine; nickel; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: Hydrogenation / 2: Tosylation / 3: cyclocondensation / 4: diethoxyphosphoryl deprotection / 5: Condensation;
DOI:10.1021/jm990211i

Reference yield:

: 89561-22-8
2,6-bis(hydroxymethyl)-4-methoxypyridine

: 170862-04-1
C₆₄H₇₈N₈O₁₀S₄

Guidance literature:: Multi-step reaction with 4 steps

1: methanesulfonyl chloride, Et₃N / CH₂Cl₂

2: Cs₂CO₃ / dimethylformamide / 24 h / 65 °C

3: glac. AcOH, HBr / 2 h / 20 °C

4: K₂CO₃ / acetonitrile / 22 h / Heating

With hydrogen bromide; potassium carbonate; caesium carbonate; acetic acid; methanesulfonyl chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: Chlorination / 2: cyclocondensation / 3: diethoxyphosphoryl deprotection / 4: Condensation;
DOI:10.1021/jm990211i