Technology Process of C30H24N2O8
There total 7 articles about C30H24N2O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide monohydrate;
In
methanol;
at 20 ℃;
for 4h;
DOI:10.1021/ol201746p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanesulfonic acid / 24 h / 80 °C
2: potassium carbonate / N,N-dimethyl-formamide / 60 °C
3: lithium hydroxide monohydrate / methanol / 4 h / 20 °C
With
methanesulfonic acid; lithium hydroxide monohydrate; potassium carbonate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/ol201746p
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydride; potassium iodide / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
1.2: 80 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 20 °C
2.2: Reflux
3.1: trichlorophosphate / 20 °C / Inert atmosphere
4.1: methanesulfonic acid / 24 h / 80 °C
5.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C
6.1: lithium hydroxide monohydrate / methanol / 4 h / 20 °C
With
methanesulfonic acid; lithium hydroxide monohydrate; sodium hydride; potassium carbonate; trifluoroacetic acid; potassium iodide; trichlorophosphate;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol201746p
