C₁₇H₂₄O₅Si

Base Information

Chemical Name:C₁₇H₂₄O₅Si
CAS No.:1379659-37-6
Molecular Formula:C₁₇H₂₄O₅Si
Molecular Weight:336.46
Hs Code.:

C<sub>17</sub>H<sub>24</sub>O<sub>5</sub>Si

Synonyms:C₁₇H₂₄O₅Si

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Chemical Property of C₁₇H₂₄O₅Si

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Technology Process of C₁₇H₂₄O₅Si

There total 4 articles about C₁₇H₂₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1335224-94-6
C₁₇H₂₂O₅Si

: 1379659-37-6
C₁₇H₂₄O₅Si

Guidance literature:: With 20% palladium hydroxide on charcoal; hydrogen; In dichloromethane; at 0 ℃; for 12h; under 760.051 Torr; optical yield given as %ee; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol301191u

Reference yield:

: 57830-00-9
1-(4-methoxyphenyl)-1-methylsilacyclobutane

: 1379659-37-6
C₁₇H₂₄O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1: allyl(cyclopentadiene)palladium(II); C₃₈H₄₂NO₂P / toluene / 14 h / 10 °C

2: 20% palladium hydroxide on charcoal; hydrogen / dichloromethane / 12 h / 0 °C / 760.05 Torr / Inert atmosphere

With allyl(cyclopentadiene)palladium(II); 20% palladium hydroxide on charcoal; C₃₈H₄₂NO₂P; hydrogen; In dichloromethane; toluene;
DOI:10.1021/ol301191u

Reference yield:

: 251453-07-3
1-chloro-1-(4'-methoxyphenyl)silacyclobutane

: 1379659-37-6
C₁₇H₂₄O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; diethyl ether / 38.5 h / 0 - 35 °C / Inert atmosphere

2: allyl(cyclopentadiene)palladium(II); C₃₈H₄₂NO₂P / toluene / 14 h / 10 °C

3: 20% palladium hydroxide on charcoal; hydrogen / dichloromethane / 12 h / 0 °C / 760.05 Torr / Inert atmosphere

With allyl(cyclopentadiene)palladium(II); 20% palladium hydroxide on charcoal; C₃₈H₄₂NO₂P; hydrogen; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ol301191u