4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)-N-isopropylaniline

Base Information

Chemical Name:4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)-N-isopropylaniline
CAS No.:1565797-10-5
Molecular Formula:C₂₂H₂₄N₂O₂S
Molecular Weight:380.511
Hs Code.:

Synonyms:4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)-N-isopropylaniline

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Chemical Property of 4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)-N-isopropylaniline

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Technology Process of 4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)-N-isopropylaniline

There total 5 articles about 4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)-N-isopropylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1565798-02-8
4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)aniline

: 75-26-3
isopropyl bromide

: 1565797-10-5
4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)-N-isopropylaniline

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 62306-04-1
2-methyl-5,6-dimethoxy-1,3-benzothiazole

: 1565797-10-5
4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)-N-isopropylaniline

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 2 h / Reflux

2.1: 2 h / 100 °C

3.1: sodium methylate / N,N-dimethyl-formamide / 0.5 h / 0 °C

3.2: 0.5 h

4.1: iron; ammonium chloride / ethanol; water / 0.5 h / Reflux

5.1: triethylamine / dichloromethane / 1 h / 20 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium methylate; iron; ammonium chloride; triethylamine; In tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 3.2: |Wittig Olefination;

Reference yield:

: 1565797-99-0
2-(bromomethyl)-5,6-dimethoxybenzo[d]thiazole

: 1565797-10-5
4-((1E,3E)-4-(5,6-dimethoxybenzo[d]thiazole-2-yl)buta-1,3-dienyl)-N-isopropylaniline

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2 h / 100 °C

2.1: sodium methylate / N,N-dimethyl-formamide / 0.5 h / 0 °C

2.2: 0.5 h

3.1: iron; ammonium chloride / ethanol; water / 0.5 h / Reflux

4.1: triethylamine / dichloromethane / 1 h / 20 °C

With sodium methylate; iron; ammonium chloride; triethylamine; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; 2.2: |Wittig Olefination;