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Technology Process of RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)(1+)*BF4(1-)=RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)BF4

RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)(1+)*BF4(1-)=RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)BF4

Base Information
  • Chemical Name:RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)(1+)*BF4(1-)=RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)BF4
  • CAS No.:81654-86-6
  • Molecular Formula:BF4*C42H56O6P5Ru
  • Molecular Weight:999.646
  • Hs Code.:
RuH(P(OCH<sub>3</sub>)3)2(C<sub>6</sub>H<sub>5</sub>P(CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2)<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=RuH(P(OCH<sub>3</sub>)3)2(C<sub>6</sub>H<sub>5</sub>P(CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2)BF<sub>4</sub>

Synonyms:RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)(1+)*BF4(1-)=RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)BF4

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Chemical Property of RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)(1+)*BF4(1-)=RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)BF4
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Technology Process of RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)(1+)*BF4(1-)=RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)BF4

There total 1 articles about RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)(1+)*BF4(1-)=RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

tetrafluoroboric acid diethyl ether
67969-82-8

tetrafluoroboric acid diethyl ether

RuHBH<sub>4</sub>(C<sub>6</sub>H<sub>5</sub>P(CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2)
81624-51-3

RuHBH4(C6H5P(CH2CH2CH2P(C6H5)2)2)

phosphorous acid trimethyl ester
121-45-9

phosphorous acid trimethyl ester

RuH(P(OCH<sub>3</sub>)3)2(C<sub>6</sub>H<sub>5</sub>P(CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2)<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=RuH(P(OCH<sub>3</sub>)3)2(C<sub>6</sub>H<sub>5</sub>P(CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2)BF<sub>4</sub>
81654-86-6

RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)(1+)*BF4(1-)=RuH(P(OCH3)3)2(C6H5P(CH2CH2CH2P(C6H5)2)2)BF4

Guidance literature:
In tetrahydrofuran; to soln. of Ru-complex in THF at 0°C was added P(OMe)3, stirred for 10 min, HBF4*Et2O was added under N2; hexane was added, after 1 wk at room temp. ppt. was isolated, washed with hexane, dried in vac., recrystd. from acetone-hexane; elem. anal.;
DOI:10.1021/ja00378a019
upstream raw materials:

tetrafluoroboric acid diethyl ether

RuHBH4(C6H5P(CH2CH2CH2P(C6H5)2)2)

phosphorous acid trimethyl ester

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